Tin electrodeposition from sulfate solution containing a benzimidazolone derivative

Authors

  • Said Bakkali Laboratoire de Matériaux d'Electrochimie et d'Environnement, Faculté des Sciences, Université Ibn Tofail, 14000 Kenitra,
  • Abdelillah Benabida Laboratoire de Matériaux d'Electrochimie et d'Environnement, Faculté des Sciences, Université Ibn Tofa, 14000 Kenitra,
  • Mohammed Cherkaoui Laboratoire de Matériaux d'Electrochimie et d'Environnement, Faculté des Sciences, Université Ibn Tofail, 14000 Kenitra,

DOI:

https://doi.org/10.13171/mjc61/01611211149/bakkali

Abstract

Tin electrodeposition in an acidic medium in the presence of N,N’-1,3-bis-[N-3-(6-deoxy-3-O-methylD-glucopyranose-6-yl)-2-oxobenzimidazol-1-yl)]-2-tetradecyloxypropane as an additive was investigated in this work. The adequate current density and the appropriate additive concentration were determined by gravimetric measurements. Chronopotentiometric curves showed that the presence of the additive caused an increase in the overpotential of tin reduction. The investigations by cyclic voltammetry technique revealed that, in the presence and in absence of the additive, there were two peaks, one in the cathodic side attributed to the reduction of Sn2+ and the other one in the anodic side assigned to the oxidation of tin previously formed during the cathodic scan. The surface morphology of the tin deposits was studied by scanning electron microscopy (SEM) and XRD.

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Published

2016-11-22

Issue

Vol. 6 No. 2 (2017)

Section

Electrochemistry

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